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Service packages

The Danish Center for Ultrahigh-Field NMR Spectroscopy offers a series of predefined packages allowing researchers or industry partners to have quick and efficient access to NMR analysis of their samples. You will find a broad range of packages listed here and below this, you will find a detailed list of equipment and further specification of the service levels.

Once you have found the correct package for you, please request the service by clicking the bottum to the right. 

The Metabolomics package

The center offers a standard package for metabolomics with 1D proton spectra recorded as noesy1dpr, cpmg, PROJECT or simple pulse-acquire with solvent suppression. 2D experiments for identification, like TOCSY, COSY or 13C-HSQC are also available. 

The user should provide the samples in short 3 or 5 mm NMR tubes in racks suited for the Bruker Samplejet. Samples can be handled in other ways with a fee of 1,000 kr/hour for the preparation. 

Conditions
Spectrometers Bruker950 and Bruker500
Probes Cryo-probe (950) or standard TXI (950 & 500)
Service levels All
Price
Academia 2,500 kr/day (full-service), 2,000 kr/day (guided-service), 1,000 kr/day (self-service) 
Industry 7,500 kr/day

The liquid-state protein package

The center offers a package of liquid-state experiments suited for structural elucidation of proteins in solution. The package is available at 950 MHz equipped with a cryo-probe for maximum sensitivity and both hsqc or trosy based experiments are available. Prior to setting up the experiments, a discussion will define the exact experiments to conduct. 

Conditions
Spectrometers Bruker950 (Bruker700 and Bruker500)
Probes Cryo-probe (950) or standard TXI (950 & 700 & 500)
Service levels All
Price
Academia

10,000 kr/week and 2,500 kr/day thereafter (full-service), 

10,000 kr/week and 2,000 kr/day thereafter (guided-service),

5,000 kr/week and 1,000 kr/day thereafter (self-service) 

Industry 7,500 kr/day

The solid-state protein package

The center offers a package of solid-state experiments suited for structural elucidation of proteins in solids. The package is available at 950 MHz equipped with probes for either 1H or 13C detection. Prior to setting up the experiments, a discussion will define the exact experiments to conduct. 

Conditions
Spectrometers Bruker950 (Bruker700)
Probes MAS 1.9mm, MAS 3.2 mm, MAS 0.7 mm (950) or MAS 1.3 mm, MAS 2.5 mm, MAS 4 mm (700)
Service levels All
Price
Academia

10,000 kr/week and 2,500 kr/day thereafter (full-service), 

10,000 kr/week and 2,000 kr/day thereafter (guided-service),

5,000 kr/week and 1,000 kr/day thereafter (self-service) 

Industry 7,500 kr/day

The solid-state materials package

The center offers a package of solid-state experiments suited for characterization of solid materials. The package is available at 950 MHz equipped with probes for low-gamma nuclei, 1H detection or medium-fast MAS. Prior to setting up the experiments, a discussion will define the exact experiments to conduct. 

Conditions
Spectrometers Bruker950
Probes Low-gamma 4 mm MAS, MAS 1.9mm (950) 
Service levels All
Price
Academia

3000 kr/day (full-service), 

2,000 kr/day (guided-service),

1,000 kr/day (self-service) 

Industry 7,500 kr/day

The Organic molecules package

The center offers a standard package for the characterization of molecules in organic solvents. A series of experiments including a long 13C, DEPT, 1H-COSY, 1H-13C HSQC, 1H-13C HMBC will be conducted. Other standard Bruker experiments can easily be added or substituted in. 

The user should provide the samples in 5 mm NMR tubes or in a relevant deuterated solvent for NMR. 

Conditions
Spectrometers Bruker950 and Bruker500
Probes Cryo-probe (950) or standard TXI (950 & 500)
Service levels All
Price
Academia 2,500 kr/day (full-service), 2,000 kr/day (guided-service), 1,000 kr/day (self-service) 
Industry 7,500 kr/day

The exploratory package

This package allows the customer test whether their samples are applicable with NMR analysis. The package is not dedicated to specific NMR method but includes support from the NMR specialist for the full period. This package allows customers to test samples before engaging in any of the other packages or before starting a scientific collaboration with any of the NMR groups involved.

Before any measurements are conducted, the NMR specialist will discuss with the customer how the testing will be performed and which results the customer is looking for.

Conditions
Spectrometers All
Probes All
Service levels Full service or Guided self-service
Price
Academia 4,000 kr/day; 2,000 kr for 4 hours
Industry 10,000 kr/day