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Near Ambient Pressure X-ray Photoelectron Spectroscopy

What is NAP-XPS?

The NAP-XPS facility at iNANO, Aarhus University, provides advanced surface chemical analysis under near-realistic environmental conditions. It is designed for researchers who want to investigate the chemistry of functional materials, interfaces, and reactive surfaces in situ, operando, or after controlled sample treatment. 

Operating at pressures up to 20 mbar, the system is equipped with dual Aluminium and Chromium X-ray sources for versatile spectral capability and an analysis depth of approximately 10–30 nm. The platform also includes a directly coupled glove box for preparing air-sensitive samples and a vacuum suitcase for contamination-free sample transfer.

Why use NAP-XPS?

NAP-XPS makes it possible to follow chemical changes at surfaces and interfaces under conditions that are much closer to real operation than conventional ultra-high-vacuum XPS. This enables molecular-level insight into reaction intermediates, interfacial chemistry, degradation processes, and surface composition in complex material systems.

Applications

  • Catalysis:

     operando probing of catalytic sites and intermediates

  • Batteries & energy storage

     in situ electrode interface and degradation analysis

  • Polymers

     real-time monitoring of chemical changes and degradation

  • Corrosion & surface protection

     evaluation of corrosion dynamics and coating performance

  • Biological material

     surface analysis of tissues, cells, and biomaterials

  • Food science

     composition assessment of food surfaces and packaging

Availability and Access

  • Access granted after review and approval of a short project description
  • Open to Aarhus University and external collaborators
  • Available from May 2026, pending project description approval
  • Early contact recommended for access arrangements
  • Inert atmosphere sample preparation with integrated glove box
  • Contamination-free sample transfer via vacuum suitcase
  • Flexible scheduling and customizable electrochemical cells